| Beamline Components | ||
| Precision Roller Jacks | Mass Spectrometer System | X-Ray Slits |
| Levels | Filter and Metal Foil Sets | NIST Standard Reference Materials |
| Precision Roller Jacks | |
| ADC Precision Crossed Roller Jacks | |
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Detector Pool has one unit available for loan. |
| Model DJ400-50 | |
| Precision jacks feature stepper motor actuation, crossed-roller bearings, Acme thread leadscrew, black anodized aluminum structure, stainless steel hardware, and up and down limit switches. Crossed-roller bearings guarantee maximum rigidity and straightness of trajectory. | |
| Dimensions in. (mm) | |
| A: 4.67 (119.1) | |
| B: 7.5 (190.5) | |
| C MIN: 17.3 (438.6) | |
| C MAX: 25.0 (635.8) | |
| D: 3.75 (95.25) | |
| E: 1.88 (47.63) | |
| F: 1.14 (35.72) | |
| DB9 Pin Assignments | |
| Mass Spectrometer System | |
| Dycor LC-Series Mass Spectrometer System | |
|
Detector Pool has one unit available for loan. |
| Dycor LC100M Mass Spectrometer | |
| Includes LC-Series Power Supply, Electrometer and Analyzer head with the following features. | |
| 1-100 AMU range | |
| Open Ion Source | |
| Faraday Cup Detector | |
| Channel Plate Electron Multiplier | |
| Rs-232 Port | |
| Dylink32 interface software | |
| System 200 Software | |
| M240 Pressure Reduction Inlet Manifold | |
| Includes all-metal, high conductance valve, bypass valve, and aperture. | |
| VPS700 Dry Pumping System | |
| ncludes wide-range turbomolecular pumping station with an Alcatel ATP 100 (70 l/s compound turbopump) controlled by an Alcatel ACP 200 T controller. | |
| Alcatel ACP28 Dry Primary Pump | |
| Peak pumping speed | |
| 27m^3/h | |
| (16cfm) | |
| X-ray Slits | |
| JJ X-ray Slits |
| The APS Detector pool has three different X-Ray Slits from JJ X-Ray. They can be used under the following conditions as required by JJ X-Ray | |
| If an APS beamline experiences trouble with one of the products listed below they can | |
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At this point, the APS Detector Pool will
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| The beamline responsible should then proceed to expediently ensure that repairing is possible by sending the slits etc. | |
| Once the repaired products have been returned the beamline responsible should return the products so that they may be ready for other users. At this point in time both the beamline and the APS Detector Pool will email JJ X-Ray that the slits have in fact been returned. | |
| JJ X-Ray Home Page | |
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| JJ X-Ray ESRF High Precision Miniature Slit | JJ X-Ray Slit Type3(air version) | JJ X-Ray Slit Type 3(vacuum version) |
| Blade Material: Tungsten Carbide sub-micro type 6 UF (corn size 0.4 micron) 2mm thick Knife edge: 2 degrees | Blade Material: Tungsten Carbide, edge with radius=16 mm on side 1 0.5 deg knife edge on side 2 | Blade Material: Tungsten Carbide, edge with radius=16 mm/ 0.5 deg. knife edge |
| Dimenations: 1113 mm by 113 mm by 45 mm | Dimenations: 95 mm by 95 mm by 50 mm | Dimenations:120 mm by 120 mm by 64 mm |
| Outer Surface: Chemical Nickel | Outer Surface: Anodized Aluminium | Outer Surface: Anodized Aluminium |
| Aperture size: 6 mm by 6mm (maximum) | ||
| Translation Range: +/- 7mm | Translation Range: +/- 13mm | Translation Range: +/-14mm |
| Resolution: Aperture: 0.8 micron in Full Step Translation: 0.3 micron in Full step | Resolution: 1mm = 1000 full steps | Resolution: 1mm = 1000 full steps |
| Repeatability: <1 micron (Unidirectional) | Repeatability: ± 1.0 micron (Unidirectional) ± 3.0 micron (Bi-directional) | Repeatability: ± 1.0 micron (Unidirectional) ± 3.0 micron (Bi-directional) |
| Absolute Accuracy: +/- 3 micron | Absolute Accuracy:> ± 2 micron (over 3 mm) | Absolute Accuracy: ± 2 micron (over 3 mm) |
| Motors: Amp. 0.45/phase (please note the low current) Aperture: Stepper 0,4 micron/half step Translation: 0.15 micron/half step | Motors: Vexta type 1PK244M-01B, 0.9 deg step angle, 3.3 ohm, 1.2 amp | Motors: Stepper motor, 0.9 deg step angle, 4VDC, 1.2 amp |
| Guiding: Precision ball slides | ||
| Electrical Connection: Male 15 pins Sub-D | Electrical Connection:Cable Diagram | Electrical Connection:Cable Diagram |
| End Stop: Microswitches electrically coupled to the 15 pins Sub-D connector | End Stop: 8 pieces micro switch | End Stop: 2*4 pieces micro switches coupled to the 2 motor Sub-D15 connectors |
| Weight: ~1 kg | Weight: ~3 kg | Weight: ~3 kg |
| Vacuum Option: Vac. Connection: 10^-5 mbar Operation - Completely inside vacuum chamber (not in EOS Equipment Pool inventory). | ||
| ESRF High Precision Miniature Slit Assembly drawing | JJ X-Ray Slit Type 3 (air verson) sketch | JJ X-Ray Slit Type 3 (vacuum verson) sketch |
| Levels | |||
| LEICA NA730 Automatic Level | |||
| Dectector Pool has 2 units available for loan. | |||
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Accuracy | ||
| Per km doulble run | 1.2mm | ||
| Single measurement – Target distance 30m | 0.8 mm | ||
| Compensator | |||
| Setting accuracy | < 0.3 | ||
| Working range | ± 15' | ||
| Enviroment | |||
| Impact standard | ISO 9022-33-5 | ||
| Resistance to water and dust ingress | IP57 | ||
| Temperature Range | |||
| - Operation | -20° to +50°C | ||
| - Storage | -40° to +70°C | ||
| Dimensions & Weight | |||
| Dimensions | 21x12x12 cm | ||
| Weight | 1.7kg | ||
| Stand | |||
| Samson | |||
| Leica GeoSystems website | |||
| Leica NA730 Datasheet | |||
| Leica NA730 Users Manual | |||
| Survey Reference Material | |||
| Wild Heerbrugg N3 Level | |||
| The Wild Heerbrugg level plus survey stand is available for loan | |||
| Detector Pool has 1 available for loan. | |||
| Accuracy | |||
| Standard deviation for 1km double run levelling | 0.2mm | ||
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Telescope, w/panfocal optics | erect image | |
| Clear objective aperture | 52mm | ||
| Magnification (decreases at short distances) | 11x@0.4 16x@1m 34x@10m 42x@100m |
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| Field of view at 100m / 1m | 1.80m / 5cm | ||
| Shortest focusing distance | .45m | ||
| Tubular level, sensitivity per 2mm | 10" | ||
| Setting accuracy (split bubble) | 0.25" | ||
| Circular level, sensitivity per 2mm | 2' | ||
| Tilting screw with graduation | 8 Revolutions | ||
| Range = 8revs = 400 intervals (400:100000) | 4.00mm / 1m (824’’) | ||
| 1 revolution = 50 intervals (50:100000) | 0.50mm / 1m (103’’) | ||
| 1 interval of drum (1:100000) | 0.01mm / 1m (2’’) | ||
| Range = 8revs = 400 intervals (400:100000) | 4.00mm / 1m (824’’) | ||
| NIST Standard Reference Materials | ||||||||
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The Equipment Pool has obtained quantities of Standard Reference Materials from NIST SRMs 640c, 660a, and 675 consist of materials with select crystallographic and microstructure properties used in the evaluation of diffraction equipment for the following variables:
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| NIST Standard Reference Materials | ||||||||
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SRM | Type | MSDS | Certificate | XRD Application | Lattice Parameters (in nm) |
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| 640 | Silicon Powder 2q/d-spacing |
640c MSDS |
640c Certificate |
Line Position |
(0.54311946 ± 0.00000092) |
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| 660a | Lanthanum Hexaboride Powder |
660a MSDS |
660a Certificate |
Quantitative Analysis |
(0.41569162 ± 0.00000097) |
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| 675 | Mica | 675 MSDS Page 1 Page 2 Page 3 Page 4 |
675 Certificate Page 1 Page 2 |
Line Position- low 2q |
0.998104 | |||
| Filter and Metal Foil Sets | |||
| X-Ray Fluorescent Filter Set | |||
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EXAFS Materials has developed a process for fabricating large-area filters of uniform thickness. Each filter is mounted in an Aluminum frame, 10 cm x 10 cm. They are sized to fit the Lytle Detector manufactured by the EXAFS COMPANY, Eagle Valley, HC 74 Box 236, Pionce, NV, 89043. |
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| X-Ray Fluorescent Filter Set | |||
| Metal | Thickness: 3 abs. lengths |
Thickness: 6 abs. lengths |
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| Ti | 90 | 100 | |
| V | 90 | 100 | |
| Cr | 90 | 100 | |
| Mn | 90 | 100 | |
| Fe | 90 | 100 | |
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Co | 90 | 100 |
| Ni | 90 | 100 | |
| Cu | 90 | 100 | |
| Zn | 90 | 100 | |
| Ga | 90 | 100 | |
| Ge | 90 | 100 | |
| As | 90 | 100 | |
| Se | 90 | 100 | |
| Zr | 150 | 180 | |
| Mo | 150 | 180 | |
| Special Filters | |||
| Metal | Thickness: 6 abs. lengths | ||
| Sr | 300 | ||
| Y | 150 | ||
| Ag | 200 | ||
| Ru | 400 | ||
| In | 180 | ||
| X-Ray 3d and 4d/5d Metal Foil Sets: | ||
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These foil sets are comprised of a series of ultra-thin 3d, 4d and 5d metal foils as standards for EXAFS and XANES measurement. Each 3d foil is approximately 5 microns thick (to give approximately 1.5 absorption lengths above the K-edge) and is mounted in individual electroplated Aluminum frames, 2.6 cm x 4.6 cm in size. The foil area is approximately 1 cm x 3 cm. The 4d and 5d foils have a greater thickness. |
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| This set of foils was purchased from 871 El Cerro Blvd Danville, CA 94526 exafs_materials@sbcglobal.net |
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| 3d Metal Foils | ||
| Metal | Thickness | |
| Ti | 6 um | |
| V | 5 um | |
| Cr | 1 um | |
| Mn | -325 mesh | |
| Fe | 7.5um | |
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| Co | 6 um | |
| Se | -325 mesh | |
| Ni | 6 um | |
| Cu | 7.5 um | |
| Zn | 17 um | |
| 4d and 5d Metal Foils | ||
| Metal | Thickness | |
| Zr | 20 um | |
| Nb | 25 um | |
| Mo | 15 um | |
| Ag | 25 um | |
| Pd | 25 um | |
| Sn | 50 um | |
| Sb | -325 mesh | |
| Au | 5 um | |
| Pb | 12 um | |
| Pt | 5 um | |
| Ta | 5 um | |
| As | -325 mesh | |
| EXAFS Materials Reference X-Ray Spectra | ||